Distillation Troubleshooting

Author: Henry Z. Kister  

Publisher: John Wiley & Sons Inc‎

Publication year: 2010

E-ISBN: 9780471690719

P-ISBN(Hardback):  9780471467441

Subject: TQ028.3 Single phase liquid mixture separation process

Language: ENG

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Description

THE FIRST BOOK OF ITS KIND ON DISTILLATION TECHNOLOGY

The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly enhanced tower capacity and efficiency. With all these advances, one would expect the failure rate in distillation towers to be on the decline. In fact, the opposite is the case: the tower failure rate is on the rise and accelerating.

Distillation Troubleshooting collects invaluable hands-on experiences acquired in dealing with distillation and absorption malfunctions, making them readily accessible for those engaged in solving today's problems and avoiding tomorrow's. The first book of its kind on the distillation industry, the practical lessons it offers are a must for those seeking the elusive path to trouble-free distillation.

Distillation Troubleshooting covers over 1,200 case histories of problems, diagnoses, solutions, and key lessons. Coverage includes:
* Successful and unsuccessful struggles with plugging, fouling, and coking
* Histories and prevention of tray, packing, and internals damage
* Lessons taught by incidents and accidents during shutdowns, commissioning, and abnormal operation
* Troubleshooting distillation simulations to match the real world
* Making packing liquid distributors work
* Plant bottlenecks from intermediate draws, chimney trays, and feed points
* Histories of and key lessons from explosions and fires in distillation towers
* Prevention of flaws that impair reboiler and condenser performance
* Destabilization of tower control systems and how to correct it
* Discoveries from shutdown inspections
* Suppression of foam and accumulation incidents

A unique resource for improving the foremost industrial separation process, Distillation Troubleshooting transforms decades of hands-on experiences into a handy reference for professionals and students involved in the operation, design, study, improvement, and management of large-scale distillation.

Chapter

Contents

pp.:  1 – 9

Preface

pp.:  9 – 25

Acknowledgments

pp.:  25 – 29

How to Use this Book

pp.:  29 – 31

Abbreviations

pp.:  31 – 33

1. Troubleshooting Distillation Simulations

pp.:  33 – 39

2. Where Fractionation Goes Wrong

pp.:  39 – 63

3. Energy Savings and Thermal Effects

pp.:  63 – 99

4. Tower Sizing and Material Selection Affect Performance

pp.:  99 – 111

5. Feed Entry Pitfalls in Tray Towers

pp.:  111 – 135

6. Packed-Tower Liquid Distributors: Number 6 on the Top 10 Malfunctions

pp.:  135 – 149

7. Vapor Maldistribution in Trays and Packings

pp.:  149 – 171

8. Tower Base Level and Reboiler Return: Number 2 on the Top 10 Malfunctions

pp.:  171 – 183

9. Chimney Tray Malfunctions: Part of Number 7 on the Top 10 Malfunctions

pp.:  183 – 201

10. Draw-Off Malfunctions (Non-Chimney Tray) Part of Number 7 on the Top 10 Malfunctions

pp.:  201 – 217

11. Tower Assembly Mishaps: Number 5 on the Top 10 Malfunctions

pp.:  217 – 231

12. Difficulties During Start-Up, Shutdown, Commissioning, and Abnormal Operation: Number 4 on the Top 10 Malfunctions

pp.:  231 – 253

13. Water-Induced Pressure Surges: Part of Number 3 on the Top 10 Malfunctions

pp.:  253 – 263

14. Explosions, Fires, and Chemical Releases: Number 10 on the Top 10 Malfunctions

pp.:  263 – 271

15. Undesired Reactions in Towers

pp.:  271 – 275

16. Foaming

pp.:  275 – 279

17. The Tower as a Filter: Part A. Causes of Plugging—Number 1 on the Top 10 Malfunctions

pp.:  279 – 291

18. The Tower as a Filter: Part B. Location of Plugging—Number 1 on the Top 10 Malfunctions

pp.:  291 – 295

19. Coking: Number 1 on the Top 10 Malfunctions

pp.:  295 – 309

20. Leaks

pp.:  309 – 319

21. Relief and Failure

pp.:  319 – 325

22. Tray, Packing, and Tower Damage: Part of Number 3 on the Top 10 Malfunctions

pp.:  325 – 329

23. Reboilers That Did Not Work: Number 9 on the Top 10 Malfunctions

pp.:  329 – 353

24. Condensers That Did Not Work

pp.:  353 – 373

25. Misleading Measurements: Number 8 on the Top 10 Malfunctions

pp.:  373 – 385

26. Control System Assembly Difficulties

pp.:  385 – 395

27. Where Do Temperature and Composition Controls Go Wrong?

pp.:  395 – 411

28. Misbehaved Pressure, Condenser, Reboiler, and Preheater Controls

pp.:  411 – 415

29. Miscellaneous Control Problems

pp.:  415 – 433

DISTILLATION TROUBLESHOOTING DATABASE OF PUBLISHED CASE HISTORIES

pp.:  433 – 435

References

pp.:  435 – 687

Index

pp.:  687 – 707

About the Author

pp.:  707 – 751

LastPages

pp.:  751 – 751

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