Newer Methods of Preparative Organic Chemistry V2

Author: Foerst   Wilhelm  

Publisher: Elsevier Science‎

Publication year: 2012

E-ISBN: 9780323150422

P-ISBN(Paperback): 9780123956484

P-ISBN(Hardback):  9780123956484

Subject: O621.3 Organic synthesis chemistry.

Language: ENG

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Description

Newer Methods of Preparative Organic Chemistry, Volume II focuses on several improved methods in preparative organic chemistry. This book presents a variety of detailed laboratory procedures in organic chemistry.
Organized into 14 chapters, this volume starts with an overview of the compound acetoacetaldehyde, which is prepared from sodium formylacetone with acetic anhydride in ether. This text then explains the requirements I a rational peptide synthesis, including controlled reaction conditions, retention of optical activity, high yields, and analogous applicability to free amino acids and to terminal amino acids of oligopeptides. Other chapters consider the general equation of the inner anhydride of acetic acid. This book discusses as well the relation between polarity and reactivity in phosphines. The final chapter deals with the methylation of aromatic compounds, which is a typical radical reaction.
This book is intended for synthetic organic chemists. Graduate students and research workers in the fields of organic chemistry and biochemistry will find this book useful.

Chapter

Front Cover

pp.:  1 – 4

Copyright Page

pp.:  5 – 12

Contributors to Volume II

pp.:  6 – 8

Preface

pp.:  8 – 10

Foreword

pp.:  10 – 16

Table of Contents

pp.:  12 – 6

Contents of Volume III

pp.:  16 – 18

Chapter 2. Preparation of Peptides and Ureas Using Reactive Amides or Imides

pp.:  48 – 68

Chapter 3. The Preparation of Long-Chain Carboxylic Acids from 1,3-Cyclohexanediones

pp.:  68 – 118

Chapter 4. Ethyl 2-Cyclopentanonecarboxylate and Its Importance in Syntheses

pp.:  118 – 150

Chapter 5. Ketene in Preparative Organic Chemistry

pp.:  150 – 180

Chapter 6. Preparative and Analytical Importance of Phosphines and Related Compounds

pp.:  180 – 230

Chapter 7. Reduction of Carbonyl Compounds with Complex Hydrides

pp.:  230 – 244

Chapter 8. Alkylation of Aromatic Amines

pp.:  244 – 270

Chapter 9. Chemical Synthesis of Intermediates of Carbohydrate Metabolism

pp.:  270 – 294

Chapter 10. Amidomethylation

pp.:  294 – 320

Chapter 11. Selective Catalytic Oxidations with Noble Metal Catalysts

pp.:  320 – 354

Chapter 12. Alkylation of Phenols with Alkenes

pp.:  354 – 378

Chapter 13. Continuous Preparation of Phenylsodium

pp.:  378 – 384

Chapter 14. Newer Investigations on Oxidation with Lead Tetraacetate

pp.:  384 – 406

Author Index

pp.:  406 – 426

Subject Index

pp.:  426 – 435

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