Trace Metal Analysis and Speciation ( Volume 47 )

Publication series :Volume 47

Author: Krull   I. S.  

Publisher: Elsevier Science‎

Publication year: 1991

E-ISBN: 9780080858548

P-ISBN(Paperback): 9780444882097

P-ISBN(Hardback):  9780444882097

Subject: O614 the metalic compound

Language: ENG

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Description

The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples.


The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in e

Chapter

Front Cover

pp.:  1 – 4

Copyright Page

pp.:  5 – 12

Preface

pp.:  6 – 10

List of Contributors

pp.:  10 – 18

CONTENTS

pp.:  12 – 6

Chapter 1. Chromatography-Element Selective Detection: Interfacing of gas-chromatography with microwave induced plasma emission detection (GC-MIP)

pp.:  18 – 38

Chapter 2. Determination of organometallic compounds in environmental samples with element-specific detectors

pp.:  38 – 66

Chapter 3. Chromatographic sample introduction for plasma mass spectrometry

pp.:  66 – 92

Chapter 4. The future of intelligent spectrometers in speciation by atomic emission spectrometry

pp.:  92 – 118

Chapter 5. Inductively coupled plasma-mass spectrometry for element-selective detection in liquid chromatography

pp.:  118 – 140

Chapter 6. The use of complexing eluents for the high performance liquid chromatographic determination of metal species

pp.:  140 – 184

Chapter 7. Instrumentation and procedures for the long term moni- toring of metal ions in industrial effluents by liquid chromatography with electrochemical detection

pp.:  184 – 230

Chapter 8. Ion chromatographic speciation of trace metals

pp.:  230 – 256

Chapter 9. Interfacing of GC/HPLC with direct current plasma (DCP) emission spectroscopic detection for trace metal analysis and speciation

pp.:  256 – 306

Subject Index

pp.:  306 – 320

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