Quality Assurance for Environmental Analysis :Method Evaluation within the Measurements and Testing Programme (BCR) ( Volume 17 )

Publication subTitle :Method Evaluation within the Measurements and Testing Programme (BCR)

Publication series :Volume 17

Author: Maier   E. A.;Griepink   B.;Quevauviller   Ph.  

Publisher: Elsevier Science‎

Publication year: 1995

E-ISBN: 9780080540078

P-ISBN(Paperback): 9780444899552

P-ISBN(Hardback):  9780444899552

Subject: X132 environmental analytical chemistry

Language: ENG

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Description

Quality assurance (QA) for environmental analysis is a growing feature of the nineties as is illustrated by the number of QA guidelines and systems which are being implemented nowadays. There is, however, often a huge gap between the implementation and respect of QA guidelines and the technical approach undertaken to improve and validate new analytical methods. This is particularly true for complex determinations involving multi-step methodologies such as those used in speciation and organic analyses.

Quality assurance may also be considered from the technical point of view, which is the focus of this book. The techniques used in different analytical fields (inorganic, speciation and organic analysis) are critically reviewed (i.e. discussion of advantages and limitations) and existing tools for evaluating their performance are described (e.g. interlaboratory studies, use of certified reference materials). Particular reference is made to the activities of the Measurements and Testing Programme (BCR) of the European Commission towards the improvement of quality control of environmental analysis.

The book has been written by experienced practitioners. By its nature, it serves as a practical reference for postgraduate students and environmental chemists who need a wide overview of the techniques used in environmental analysis and existing ways of evaluating the performance of relevant analytical methods. The critical discussions of the methods described, as well as the develo

Chapter

Cover

pp.:  1 – 6

Contents

pp.:  6 – 20

Preface

pp.:  20 – 22

Chapter 2. Isotope Dilution analysis and ICP-MS: an analyst's dream ?

pp.:  48 – 60

Chapter 3. Detection of sources of error in the determination of Cr in environmental matrices by FAAS and ETAAS

pp.:  60 – 84

Chapter 4. Analysis of environmental and biological samples by atomic spectroscopic methods

pp.:  84 – 110

Chapter 5. Validation of Neutron Activation Analysis Techniques

pp.:  110 – 132

Chapter 6. Flow-through (bio)chemical sensors in environmental analysis

pp.:  132 – 186

Chapter 7. Fiber optical sensors applied to field measurements

pp.:  186 – 216

Chapter 8. Chromium speciation in enviromnental and biological samples

pp.:  216 – 236

Chapter 9. Determination of aluminium species in natural waters

pp.:  236 – 256

Chapter 10. Selenium speciation analyses in water and sediment matrices

pp.:  256 – 284

Chapter 11. Antimony speciation in water

pp.:  284 – 306

Chapter 12. Arsenic speciation in environmental matrices

pp.:  306 – 326

Chapter 13. Mercury speciation in biological matrices

pp.:  326 – 340

Chapter 14. Speciation analysis of organolead compounds. Status and future prospects

pp.:  340 – 378

Chapter 15. Speciation analysis of organotin by GC-AAS and GC-AES after extraction and derivatization

pp.:  378 – 432

Chapter 16. High performance liquid chromatography - isotope dilution - inductively coupled plasma - mass spectrometry for lead and tin speciation in environmental samples

pp.:  432 – 456

Chapter 17. Speciation of organotin compounds in environmental samples by GC-MS

pp.:  456 – 486

Chapter 18. Development of supercritical fluid extraction procedures for the determination of organotin compounds in sediment

pp.:  486 – 510

Chapter 19. Hydride generation for speciation analyses using CG/AAS

pp.:  510 – 526

Chapter 20. Single and sequential extraction schemes for trace metal speciation in soil and sediment

pp.:  526 – 546

Chapter 21. Methods for the determination of chlorinated biphenyls in air

pp.:  546 – 556

Chapter 22. Sample handling and determination of carbamate pesticides and their transformation products in various matrices

pp.:  556 – 584

Chapter 23. Method development for the determination of polycyclic aromatic hydrocarbons (PAHs) in environmental matrices

pp.:  584 – 612

Chapter 24. Method validation for the determination of dioxins

pp.:  612 – 662

Subject index

pp.:  662 – 671

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