Basic Techniques of Preparative Organic Chemistry

Author: Sabel   William;Robinson   Robert  

Publisher: Elsevier Science‎

Publication year: 2013

E-ISBN: 9781483213774

P-ISBN(Paperback): 9780080123073

P-ISBN(Hardback):  9780080123073

Subject: O62 Organic Chemistry

Language: ENG

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Description

Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.

Chapter

Chapter 1. General Introduction

The Nature of Organic Reactions

Basic Principles of Preparative Organic Chemistry

Unit Operations

Reports and Communications

Good Laboratory Practice

Yields and Losses—Their Calculation and Importance

Chapter 2. Review of Apparatus and Equipment

Glassware

Ground-glass Fittings

Corks and Bungs

Size of Apparatus: Flasks

Separating funnels

Cleaning and Drying Glassware

Chapter 3. Hazards

Toxicity

Bodily Injuries

Smoking

Fire

Explosion

Implosion

General Attitude to Hazards

Chapter 4. Techniques and Unit Operations for Carrying Out a Reaction

General Principles

Materials Handling

Assembly of Apparatus

Heat Transfer

Chapter 5. Techniques and Unit Operations for Isolating and Purifying a Reaction Product

Distillation

Extraction

Recrystallization

Precipitation

Filtration

Chapter 6. Drying

Solids

Liquids

Gase

Chapter 7. Criteria of Purity

Determination of a Melting Point

Mixed Melting Points

Refractive Index

Chromatography

Chapter 8. Packing and Storing Products and Samples

Solids

Liquids

Labels for Samples, etc.

Chapter 9. Reports and Communications

APPENDIX: Specimen Laboratory Notebook Records

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