Analytical Methods for Food Safety by Mass Spectrometry ：Volume I Pesticides

Publication subTitle ：Volume I Pesticides

Author： Pang Guo-Fang

Publisher： Elsevier Science‎

Publication year： 2018

E-ISBN: 9780128141687

P-ISBN(Paperback): 9780128141670

Subject： S859.84 chemical residues in food of animal origin

Keyword：分析化学,仪器分析法（物理及物理化学分析法）,物理学

Language： ENG

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Description

Analytical Methods for Food Safety by Mass Spectrometry, Volume One: Pesticides systematically introduces the Pesticide and Veterinary Drug Multiresidues Analytical Methods. Volume One includes discussions on 20 pesticide multiresidues chromatic-MS (GC-MS and LC-MS/MS) analytical techniques that have the capability of detecting over 800 pesticides and chemicals in 10 categories of agricultural products, including fruits, vegetables, grains, teas, Chinese medicinal herbs, edible fungus mushrooms, fruit and vegetable juices, animal tissues, aquatic products, raw milk and milk powders, and drinkable water. This book also includes chromatic-MS analytical parameters, linear equations and GPC chromatic behavior parameters for over 800 pesticides.

This valuable book can be used as reference for not only university students, but also technical personnel of different specialties who are engaged with study and applications, such as food safety, agricultural environment protection, pesticide development, and utilization in scientific research units, institutions and quality inspection organizations.

Provides the chromatic-MS analytical technique for over 1000 commonly-used veterinary and pesticide residues
Covers a large varieties of target compounds, including over 800 pesticides (organophosphorus, organochlorine, carbamate, pyrethroids) and over 200 veterinary drugs, including Fluoroquinolone, Sulfonamides, Chloramphenicol, Nitrofurans, Tetracycline

Chapter

Front Cover

Analytical Methods for Food Safety by Mass Spectrometry: Volume I Pesticides

Contents

Main Researchers/Editors

Preface

Brief Introduction

Chapter 1: Introduction

1.1. Insecticides

1.1.1. Organophosphate Insecticides

1.1.2. Carbamate Insecticides

1.1.3. Organochlorine Insecticides

1.1.4. Pyrethroid Insecticides

1.1.5. Neonicotinoid Insecticides

1.2. Herbicides

1.2.1. Phenolic Herbicides

1.2.2. Phenoxy Acid Herbicides

1.2.3. Benzoic Acid Herbicides

1.2.4. Diphenyl Ether Herbicides

1.2.5. Dinitroaniline Herbicides

1.2.6. Amide Herbicides

1.2.7. Carbamate Herbicides

1.2.8. Thiocarbamate Herbicides

1.2.9. Urea Herbicides

1.2.10. Sulfonylurea Herbicides

1.2.11. S-Triazine Herbicides

1.2.12. Quaternary Ammoniums Herbicides

1.2.13. Organophosphate Herbicides

1.2.14. Other Herbicides

1.3. Bactericides

1.3.1. Triazole Bactericides

1.3.2. Amide Bactericides

1.3.3. Pyridinamine Bactericides

1.3.4. Strobin Bactericides

1.3.5. Oxazo Bactericides

1.3.6. Pyrrole Bactericides

1.3.7. Amino Acid Bactericides

1.3.8. Derivants of Cinnamic Acid

1.3.9. Others

1.4. Pesticides Banned in the World

1.4.1. Pesticides Banned in China

1.4.2. Pesticides Banned in Japan

1.4.3. Pesticides Banned in European Union

Chapter 2: Analytical Methods for 793 Pesticides and Related Chemical Residues in Products of Plant Origin

2.1. Determination of 512 Pesticides and Related Chemical Residues in Fruit Juice and Wine: LC-MS-MS METHOD (GB/T 23206-2008)

2.1.1. Scope

2.1.2. Principle

2.1.3. Reagents and Materials

2.1.4. Apparatus

2.1.5. Sample Pretreatment

2.1.5.1. Preparation of Test Sample

2.1.5.2. Extraction

2.1.5.3. Clean-up

2.1.6. Determination

2.1.6.1. LC-MS-MS Operating Condition

Conditions for the Pesticides and Related Chemicals of A, B, C, D, E, and F Groups

Conditions for the Pesticides and Related Chemicals of G Group

2.1.6.2. Qualitative Determination

2.1.6.3. Quantitative Determination

2.1.6.4. Parallel Test

2.1.6.5. Blank Test

2.1.7. Precision

Researchers

2.2. Determination of 500 Pesticides and Related Chemical Residues in Fruits and Vegetables: GC-MS Method (GB/T 19648-2006)

2.2.1. Scope

2.2.2. Principle

2.2.3. Reagents and Materials

2.2.4. Apparatus

2.2.5. Sample Pretreatment

2.2.5.1. Preparation of Test Sample

2.2.5.2. Extraction

2.2.5.3. Clean-up

2.2.6. GC-MS Determination

2.2.6.1. GC-MS Operating Condition

2.2.6.2. Qualitative Determination

2.2.6.3. Quantitative Determination

2.2.6.4. Parallel Test

2.2.6.5. Blank Test

2.2.7. Precision

Researchers

2.3. Determination of 450 Pesticides and Related Chemical Residues in Fruits and Vegetables: LC-MS-MS METHOD (GB/T 20769-2008)

2.3.1. Scope

2.3.2. Principle

2.3.3. Reagents and Materials

2.3.4. Apparatus

2.3.5. Sample Pretreatment

2.3.5.1. Preparation of Test Sample

2.3.5.2. Extraction

2.3.5.3. Clean-up

2.3.6. Determination

2.3.6.1. LC-MS-MS Operating Conditions

Operating Conditions for the Pesticides and Related Chemicals of A, B, C, D, E, and F Group

Operating Conditions for the Pesticides and Related Chemicals of G Group

2.3.6.2. Qualitative Determination

2.3.6.3. Quantitative Determination

2.3.6.4. Parallel Test

2.3.6.5. Blank Test

2.3.7. Precision

Researchers

2.4. Determination of 475 Pesticides and Related Chemical Residues in Grains: GC-MS method (GB/T 19649-2006)

2.4.1. Scope

2.4.2. Principle

2.4.3. Reagents and Materials

2.4.4. Apparatus

2.4.5. Sample Pretreatment

2.4.5.1. Preparation of Test Sample

2.4.5.2. Extraction

2.4.5.3. Clean-up

2.4.6. GC-MS Method Determination

2.4.6.1. GC-MS Operating Condition

2.4.6.2. Qualitative Determination

2.4.6.3. Quantitative Determination

2.4.6.4. Parallel Test

2.4.6.5. Blank Test

2.4.7. Precision

Researchers

2.5. Determination of 486 Pesticides and Related Chemical Residues in Grains: LC-MS-MS Method (GB/T 20770-2008)

2.5.1. Scope

2.5.2. Principle

2.5.3. Reagents and Materials

2.5.4. Apparatus

2.5.5. Sample Pretreatment

2.5.5.1. Preparation of Test Sample

2.5.5.2. Extraction

2.5.5.3. GPC Clean-up

2.5.5.3.1. Conditions

2.5.5.3.2. Clean-up

2.5.6. Determination

2.5.6.1. LC-MS-MS Operation Condition

Conditions for the Pesticides and Related Chemicals of A, B, C, D, E, and F Group (ESI Positive Ion Source)

Conditions for the Pesticides and Related Chemicals of G Group (ESI Positive Ion Source)

2.5.6.2. Qualitative Determination

2.5.6.3. Quantitative Determination

2.5.6.4. Parallel Test

2.5.6.5. Blank Test

2.5.7. Precision

Researchers

2.6. Determination of 519 Pesticides and Related Chemical Residues in Tea Leaves: GC-MS Method (GB/T 23204-2008)

2.6.1. Scope

2.6.2. Determination of 490 Pesticides and Related Chemical Residues in Tea: GC-MS Method

2.6.2.1. Principle

2.6.2.2. Reagents and Materials

2.6.2.3. Apparatus

2.6.2.4. Sample Pretreatment

2.6.2.4.1. Preparation of Test Sample

2.6.2.4.2. Extraction

2.6.2.4.3. Clean-up

2.6.2.5. Determination

2.6.2.5.1. GC-MS Operating Conditions

2.6.2.5.2. Qualitative Determination

2.6.2.5.3. Quantitative Determination

2.6.2.5.4. Parallel Test

2.6.2.5.5. Blank Test

2.6.2.6. Precision

2.6.3. Determination of 29 Acidic Herbicides in Tea: GC-MS Method

2.6.3.1. Principle

2.6.3.2. Reagents and Materials

2.6.3.3. Apparatus

2.6.3.4. Sample Pretreatment

2.6.3.4.1. Preparation of Test Sample

2.6.3.4.2. Extraction

2.6.3.4.3. Clean-up With Graphitized Carbon Black Solid Phase Extraction

2.6.3.4.4. Derivatization

2.6.3.4.5. Clean-up With Forisil Solid Phase Extraction

2.6.3.5. Determination

2.6.3.5.1. GC-MS Operating Condition

2.6.3.5.2. Qualitative Determination

2.6.3.5.3. Quantitative Determination

2.6.3.5.4. Parallel Test

2.6.3.5.5. Blank Test

2.6.3.6. Precision

Researchers

2.7. Determination of 448 Pesticides and Related Chemical Residues in Tea Leaves: LC-MS-MS METHOD (GB/T23205-2008)

2.7.1. Scope

2.7.2. Principle

2.7.3. Reagents and Materials

2.7.4. Apparatus

2.7.5. Sample Pretreatment

2.7.5.1. Preparation of Test Sample

2.7.5.2. Extraction

2.7.5.3. Clean-up

2.7.6. Determination

2.7.6.1. LC-MS-MS Operating Condition

Determination of Conditions of Group A, B, C, D, E, F Pesticides and Related Chemicals

Determination Conditions of Group G Pesticides and Related Chemicals

2.7.6.2. Qualitative Determination

2.7.6.3. Quantitative Determination

2.7.6.4. Parallel Test

2.7.6.5. Blank Test

2.7.7. Precision

Researchers

2.8. Determination of 488 Pesticides and Related Chemical Residues in Mulberry Twig, Honeysuckle, Barbary Wolfberry Fruit ...

2.8.1. Scope

2.8.2. Principle

2.8.3. Reagents and Materials

2.8.4. Apparatus

2.8.5. Sample Pretreatment

2.8.5.1. Preparation of Test Sample

2.8.5.2. Extraction

2.8.5.3. Clean-up

2.8.6. Determination

2.8.6.1. GC-MS Operating Condition

2.8.6.2. Qualitative Determination

2.8.6.3. Quantitative Determination

2.8.6.4. Parallel Test

2.8.6.5. Blank Test

2.8.7. Precision

Researchers

2.9. Determination of 413 Pesticides and Related Chemical Residues in Mulberry Twig, Honeysuckle, Barbary Wolfberry Fruit ...

2.9.1. Scope

2.9.2. Principle

2.9.3. Reagents and Materials

2.9.4. Apparatus

2.9.5. Sample Pretreatment

2.9.5.1. Preparation of Test Sample

2.9.5.2. Extraction

2.9.5.3. Clean-up

2.9.6. Determination

2.9.6.1. LC-MS-MS Operating Conditions

Operating Conditions for Groups A, B, C, D, E, and F (ESI+)

Operating Conditions of G Group (ESI-)

2.9.6.2. Qualitative Determination

2.9.6.3. Quantitative Determination

2.9.6.4. Parallel Test

2.9.6.5. Blank Test

2.9.7. Precision

Researchers

2.10. Determination of 503 Pesticides and Related Chemical Residues in Mushrooms: GC-MS Method (GB/T 23216-2008)

2.10.1. Scope

2.10.2. Principle

2.10.3. Reagents and Materials

2.10.4. Apparatus

2.10.5. Sample Pretreatment

2.10.5.1. Preparation of Test Sample

2.10.5.2. Extraction

2.10.5.3. Clean-up

2.10.6. Determination

2.10.6.1. GC-MS Operating Condition

2.10.6.2. Qualitative Determination

2.10.6.3. Quantitative Determination

2.10.6.4. Parallel Test

2.10.6.5. Blank Test

2.10.7. Precision

Researchers

2.11. Determination of 440 Pesticides and Related Chemical Residues in Edible Fungus: LC-MS-MS METHOD (GB/T 23202-2008)

2.11.1. Scope

2.11.2. Principle

2.11.3. Reagents and Materials

2.11.4. Apparatus

2.11.5. Sample Pretreatment

2.11.5.1. Preparation of Test Sample

2.11.5.2. Extraction

2.11.5.3. Clean-up

2.11.6. Determination

2.11.6.1. LC-MS-MS Operating Condition

Operating Conditions for Group A, B, C, D, E and F

Operating Conditions for Group G

2.11.6.2. Qualitative Determination

2.11.6.3. Quantitative Determination

2.11.6.4. Parallel Test

2.11.6.5. Blank Test

2.11.7. Precision

Researchers

Chapter 3: Analytical Methods for 790 Pesticides and Related Chemical Residues in Products of Animal Origin

3.1. Determination of 511 Pesticides and Related Chemical Residues in Milk and Milk Powder: GC-MS Method (GB/T 23210-2008)

3.1.1. Scope

3.1.2. Principle

3.1.3. Reagents and Materials

3.1.4. Apparatus

3.1.5. Sample Pretreatment

3.1.5.1. Storage of Test Sample

3.1.5.2. Extraction

3.1.5.3. Clean-up

3.1.6. Determination

3.1.6.1. GC-MS Operating Conditions

3.1.6.2. Qualitative Determination

3.1.6.3. Quantitative Determination

3.1.6.4. Parallel Test

3.1.6.5. Blank Test

3.1.7. Precision

Researchers

3.2. Determination of 493 Pesticides and Related Chemical Residues in Milk and Milk Powder: LC-MS-MS METHOD (GB/T 23211-2008)

3.2.1. Scope

3.2.2. Principle

3.2.3. Reagents and Materials

3.2.4. Apparatus

3.2.5. Sample Pretreatment

3.2.5.1. Storage of Test Sample

3.2.5.2. Extraction

3.2.5.3. Clean-up

3.2.6. Determination

3.2.6.1. LC-MS-MS Operating Condition

Conditions for A, B, C, D, E, and F Groups

Conditions for G Group

3.2.6.2. Qualitative Determination

3.2.6.3. Quantitative Determination

3.2.6.4. Parallel Test

3.2.6.5. Blank Test

3.2.7. Precision

Researchers

3.3. Determination of 485 Pesticides and Related Chemical Residues in Fugu, Eel, and Prawn: GC-MS Method (GB/T 23207-2008)

3.3.1. Scope

3.3.2. Principle

3.3.3. Reagents and Materials

3.3.4. Apparatus

3.3.5. Sample Pretreatment

3.3.5.1. Preparation of Test Sample

3.3.5.2. Extraction

3.3.5.3. GPC Clean-up

3.3.5.3.1. Conditions

3.3.5.3.2. Clean-up

3.3.6. Determination

3.3.6.1. GC-MS Operating Conditions

3.3.6.2. Qualitative Determination

3.3.6.3. Quantitative Determination

3.3.6.4. Parallel Test

3.3.6.5. Blank Test

3.3.7. Precision

Researchers

3.4. Determination of 450 Pesticides and Related Chemical Residues in Fugu, Eel, and Prawn: LC-MS-MS Method (GB/T 23208-2008)

3.4.1. Scope

3.4.2. Principle

3.4.3. Reagents and Materials

3.4.4. Apparatus

3.4.5. Sample Pretreatment

3.4.5.1. Preparation of Test Sample

3.4.5.2. Extraction

3.4.5.3. GPC Clean-up

3.4.5.3.1. Conditions

3.4.5.3.2. Clean-up

3.4.6. Determination

3.4.6.1. LC-MS-MS Operating Conditions

Conditions for the Pesticides and Related Chemicals of Group A-F

3.4.6.2. Conditions for the Pesticides and Related Chemicals of Group G

3.4.6.3. Qualitative Determination

3.4.6.4. Quantitative Determination

3.4.6.5. Parallel Test

3.4.6.6. Blank Test

3.4.7. Precision

Researchers

3.5. Determination of 497 Pesticides and Related Chemical Residues in Honey, Fruit Juice, and Wine: GC-MS Method (GB/T 19 ...

3.5.1. Scope

3.5.2. Principle

3.5.3. Reagents and Materials

3.5.4. Apparatus

3.5.5. Sample Pretreatment

3.5.5.1. Preparation of Test Sample

3.5.5.2. Extraction

3.5.5.3. Clean-up

3.5.6. Determination

3.5.6.1. GC-MS Operating Condition

3.5.6.2. Qualitative Determination

3.5.6.3. Quantitative Determination

3.5.6.4. Parallel Test

3.5.6.5. Blank Test

3.5.7. Precision

Researchers

3.6. Determination of 486 Pesticides and Related Chemical Residues in Honey: LC-MS-MS METHOD (GB/T 20771-2008)

3.6.1. Scope

3.6.2. Principle

3.6.3. Reagents and Materials

3.6.4. Apparatus

3.6.5. Sample Pretreatment

3.6.5.1. Preparation of Test Sample

3.6.5.2. Extraction

3.6.5.3. Clean-up

3.6.6. Determination

3.6.6.1. LC-MS-MS Operating Condition

Conditions for the Pesticides and Related Chemicals of A, B, C, D, E and F Group

Conditions for the Pesticides and Related Chemicals of Group G

Conditions for the Pesticides and Related Chemicals of Group H

Conditions for the Pesticides and Related Chemicals of Group I

3.6.6.2. Qualitative Determination

3.6.6.3. Quantitative Determination

3.6.6.4. Parallel Test

3.6.6.5. Blank Test

3.6.7. Precision

Researchers

3.7. Determination of 478 Pesticides and Related Chemical Residues in Animal Muscles: GC-MS Method (GB/T 19650-2006)

3.7.1. Scope

3.7.2. Principle

3.7.3. Reagents and Materials

3.7.4. Apparatus

3.7.5. Sample Pretreatment

3.7.5.1. Preparation of Test Sample

3.7.5.2. Extraction

3.7.5.3. GPC Clean-up

3.7.5.3.1. Conditions

3.7.5.3.2. Clean-up

3.7.6. Determination

3.7.6.1. GC-MS Operating Conditions

3.7.6.2. Qualitative Determination

3.7.6.3. Quantitative Determination

3.7.6.4. Parallel Test

3.7.6.5. Blank Test

3.7.7. Precision

Researchers

3.8. Determination of 461 Pesticides and Related Chemical Residues in Animal Muscles: LC-MS-MS Method (GB/T 20772-2008)

3.8.1. Scope

3.8.2. Principle

3.8.3. Reagents and Materials

3.8.4. Apparatus

3.8.5. Sample Pretreatment

3.8.5.1. Preparation of Test Sample

3.8.5.2. Extraction

3.8.5.3. GPC Clean-up

3.8.5.3.1. Conditions

3.8.5.3.2. Clean-up

3.8.6. Determination

3.8.6.1. LC-MS-MS Operating Conditions

Operating Conditions of Group A, B, C, D, E, and F

Operating Conditions of Group G)

3.8.6.2. Qualitative Determination

3.8.6.3. Quantitative Determination

3.8.6.4. Parallel Test

3.8.6.5. Blank Test

3.8.7. Precision

Researchers

Chapter 4: Determination of 450 Pesticides and Related Chemical Residues in Drinking Water: LC-MS-MS Method (GB/T 23214-2008)

4.1. Scope

4.2. Principle

4.3. Reagents and Materials

4.4. Apparatus

4.5. Sample pretreatment

4.5.1. Preparation of Test Sample

4.5.2. Extraction

4.5.3. Clean-up

4.6. Determination

4.6.1. LC-MS-MS Operating Condition

4.6.1.1. LC-MS-MS Operating Conditions of A, B, C, D, E, F Group

4.6.1.2. LC-MS-MS Operating Condition of G group

4.6.2. Qualitative Determination

4.6.3. Quantitative Determination

4.7. Precision

Researchers

Chapter 5: Basic Research on Chromatography-Mass Spectroscopy Characteristic Parameters of Pesticide and Chemical Pollutants

5.1. Mass Spectrometry Data of 1200 Pesticides and Chemical Pollutants Determined by GC-MS, GC-MS-MS, and LC-MS-MS

5.1.1. Retention Times, Quantifier and Qualifier Ions of 567 Pesticides and Chemical Pollutants Determined by GC-MS

5.1.2. Monitoring of Selected Ions for 567 Pesticides and Chemical Pollutants Determined by GC-MS

5.1.3. Retention Time, Quantifier and Qualifier Ions, and Collision Energies of 454 Pesticides and Chemical Pollutants De ...

5.1.4. Monitoring of Selected Ions for 454 Pesticides and Chemical Pollutants Determined by GC-MS-MS

5.1.5. Retention Time, Quantifier and Qualifier Ions, and Collision Energies of 284 Environmental Pollutants by GC-MS-MS

5.1.6. Retention Times, Selective Ions, and Relative Abundances of Endosulfans Determined by GC-NCI-MS

5.1.7. Retention Times, Quantifying and Qualifying Ions, Declustering Potentials, and Collision Energies of 9 Environment ...

5.1.8. Retention Times, Quantifying and Qualifying Ions, Fragmentor, and Collision Energies of 569 Pesticides and Chemica ...

5.1.9. Accurate Masses, Retention Times, Parent Ions, and Collision Energies of 492 Pesticides and Chemical Pollutants De ...

5.2. Linear Equation Parameters of 1200 Pesticides and Chemical Pollutants Determined by GC-MS, GC-MS-MS, and LC-MS-MS

5.2.1. Linear Equations, Linear Ranges, and Correlation Coefficients of 567 Pesticides and Chemical Pollutants Determined ...

5.2.2. Linear Equations, Linear Ranges, and Correlation Coefficients of 466 Pesticides and Chemical Pollutants Determined ...

5.2.3. Linear Equations, Linear Ranges, and Correlation Coefficients of 284 Environmental Pollutants Determined by GC-MS-MS

5.2.4. Linear Equations, Linear Ranges, and Correlation Coefficients of Endosulfans Determined by GC-MS(NCI)

5.2.5. Linear Equations, Linear Ranges, and Correlation Coefficients of 9 Environmental Pollutants Determined by LC-MS-MS

5.2.6. Linear Equations, Linear Ranges, and Correlation Coefficients of 569 Pesticides and Chemical Pollutants Determined ...

5.3. GPC Analytical Parameters of Pesticides and Chemical Pollutants

5.3.1. GPC Analytical Parameters of 744 Pesticides and Chemical Pollutants

5.3.2. GPC Analytical Parameters of 107 Pesticides and Chemical Pollutants

Appendix A: Index of 1039 Pesticides and Chemical Pollutants Determined by GC-MS, GC-MS-MS and LC-MS-MS

Appendix B: Solvent Selected and Concentration of Mixed Standard Solution of Pesticides and Chemical Pollutants

Appendix C: Physicochemical Properties of 900 Pesticides and Chemical Pollutants

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