Description
Annual Reports on NMR Spectroscopy, Volume 94, provides a thorough accounting of progress in nuclear magnetic resonance (NMR) spectroscopy and its applications in all branches of science in which precise structural determination is required, and in which the nature of interactions and reactions in solution is being studied. Updates in this new release include sections on 31PNMR Studies of Lateral Diffusion, Progress in the Accurate Determination of 1H-1H Distances by NMR Procedures, Recent Solid State NMR Studies of Hydrated Lipid Membranes, and Recent Advances in 17O NMR Studies.
This book has established itself as a premier means for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy.
- Serves as the premier resource for learning the new techniques and applications of NMR spectroscopy
- Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules
- Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)
Chapter
2. Explaining the NOE as a Relaxation Phenomenon
3. Summary of the Methods Detecting Steric Proximities
3.1. Steady-State Applications
3.2. Transient NOE Applications
3.4. The Impact of Molecular Weight and Magnetic Field Strength-ROESY
3.5. Selective 1D Applications
4. Integration of the Spectra, Determination of the Exact Interatomic Distances
5. Structure Determination of Biopolymers
Chapter Two: Recent Solid-State NMR Studies of Hydrated Lipid Membranes
2. Basic Methods in Solid-State NMR for the Study of Hydrated Lipid Membrane Systems
2.1. 2H NMR of Lipids in Membranes
3. Lipid Rafts Formed by Sphingomyelin and Cholesterol
3.1. 2H NMR for Determining the Ordering of Acyl Chains in Lipid-Raft Model Membranes
3.2. Local Orientation and Dynamics
3.3. Lipid Composition of Phase-Separated Bilayers
4. Solid-State NMR Study of Natural Product-Lipid Interactions in Hydrated Membranes
4.1. Stable-Isotope Labelling of Target Compounds
4.2. AmB and Other Natural Product-Sterol Interactions
4.3. Structure of the AmB-Erg Complex in a Hydrated Membrane
4.4. AmB-Phospholipid Interactions
4.5. AmB-AmB Interactions
Chapter Three: Lateral Diffusion and NMR
3. Lateral Diffusion Measurement Techniques
4. NMR Spectroscopy in Membranes
5. Gradient-Based NMR Lateral Diffusion Measurements
5.2. Macroscopically Oriented Membranes
5.3. Magnetically Aligned Bicelles
6. Exchange-Based NMR Lateral Diffusion Measurements
Chapter Four: Recent Developments in NMR Studies of Aluminophosphates
2. NMR Properties of Isotopes in Aluminophosphate
2.3. NMR Properties of Other Isotopes
3. NMR Methods for the Study of Aluminophosphates
3.2. NMR Methods for Quadrupolar Nuclei
3.3. Wideline NMR Methods
3.4. Probing Connectivities and Proximities Between Identical Nuclei
3.4.1. Probing Connectivities Between Identical Nuclei
3.4.2. Probing Proximities Between Identical Nuclei
3.5. Probing Connectivities and Proximities Between Distinct Isotopes
3.5.1. Probing Connectivities Between Distinct Isotopes
3.5.2. Probing Proximities Between Distinct Isotopes
4. NMR of Crystalline Aluminophosphates
4.1. Structure Determination: NMR, Graph Theory, DFT Calculations
4.2. Localization of Water Molecules and SDAs
4.3.4. Phase Transformation
5. NMR of Aluminophosphate Glasses
5.1.1. 1D 27AL NMR Spectra
5.1.2. 1D 31P NMR Spectra
5.2.1. 31P-27Al HETCOR 2D Spectra: A Qualitative Vision of the P-O-Al Linkages
5.2.2. Quantitative Data Derived From the Measurement of 31P-27Al Dipolar Interactions
5.3. Crystallization and Dynamics in Aluminophosphate-Based Glasses From Ex Situ and High Temperature In Situ MAS-NMR
5.3.1. Crystallization of Aluminophosphate Glasses
5.3.2. Dynamics Above the Glass Transition
Chapter Five: 17O NMR as a Tool in Discrete Metal Oxide Cluster Chemistry
2. 17O as a Nucleus in Metal Oxide Cluster Chemistry
2.1. The Classical Vector Model of Nuclear Magnetic Resonance
2.3. Solvent Exchange in Paramagnetic Systems
3. Solution Dynamics of Nanometer-Sized Aqueous Cluster Ions
4.1. Mechanisms of Ligand Exchange via 17O NMR
4.2. Devices to Reach GPa Pressures for Solution NMR
5. Computation of 17O Chemical Shifts of Metal Oxide Clusters by Density Functional Theory
Annual Reports on NMR Spectroscopy
( Volume 94 )
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