Synthesis, spectroscopic investigation, crystal and molecular structure of [ReCl2(N2COPh)(C10H14N2)(PPh3)2]

Author： Michalik S.   Kruszynski R.   Leszczynska-Sejda K.   Kusz J.   Krompiec S.  

Publisher： Taylor & Francis Ltd

ISSN： 0095-8972

Source： Journal of Coordination Chemistry, Vol.62, Iss.8, 2009-01, pp. : 1232-1239

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Abstract

[ReCl2(N2COPh)(C10H14N2)(PPh3)2] has been obtained in the reaction of benzoylhydrazido-Re(V) with an excess of nicotine. The [ReCl2(N2COPh)(C10H14N2)(PPh3)2] complex crystallizes in the monoclinic space group P21/n. The complex was characterized by infrared, Ultaviolet-visible, 1H NMR and magnetic measurements.

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