

Author: Grass Robert N. Stark Wendelin J.
Publisher: Springer Publishing Company
ISSN: 1388-0764
Source: Journal of Nanoparticle Research, Vol.8, Iss.5, 2006-10, pp. : 729-736
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Abstract
Metallic bismuth nanoparticles of over 98% purity were prepared by a modified flame spray synthesis method in an inert atmosphere by oxygen-deficient combustion of a bismuth-carboxylate based precursor. The samples were characterized by X-ray diffraction, thermal analysis and scanning electron microscopy confirming the formation of pure, crystalline metallic bismuth nanoparticles. Compression of the as-prepared powder resulted in highly dense, nanocrystalline pills with strong electrical conductivity and bright metallic gloss.
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