Zinc(II) (o-hydroxybenzaldoximates) Complexes with Mono- and Bidentate Ligands

Author： Olczak-Kobza M.   Cichecka M.  

Publisher： Springer Publishing Company

ISSN： 1388-6150

Source： Journal of Thermal Analysis and Calorimetry, Vol.66, Iss.2, 2001-11, pp. : 379-386

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Abstract

New complexes: Zn(Hsalox)(ox), Zn(Hsalox)(NHPh), Zn(Hsalox)(Hsal) and Zn(Hsalox)2(1,2-diMeim) have been synthesised as a result of a reaction of Zn(salox) and Zn(Hsalox)2 (where: salox 2−=OC6H4CHNO2−, Hsalox −=OC6H4CHNOH−) with 8-hydroxyquinoline (Hox), o-aminophenol (NH2Ph), o-hydroxybenzoic acid (H2Sal) and1,2-dimethylimidazole (1,2-diMeim). Chemical, X-ray and thermal analyses of the complexes and their sinters have been carried out. Thermal decomposition pathways have been postulated for the complexes. The mixtures about not definite composition have been obtained as a result of a reaction of zinc(o-hydroxybenzaldoximates) with imidazole(Him) and 4-methylimidazole (4-MeHim).

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