Author: O'Neill Alison Turner Andrew D.
Publisher: AOAC International
E-ISSN: 1944-7922|98|3|628-635
ISSN: 1944-7922
Source: Journal of AOAC International, Vol.98, Iss.3, 2015-05, pp. : 628-635
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Abstract
An approach was developed for the verification of method performance of the AOAC 2005.06 LC-fluorescence detector (FLD) method for determination of paralytic shellfish poisoning (PSP) toxins in bivalve shellfish. This was developed following advice published by the Analytical Laboratory Accreditation Criteria Committee and applied to shellfish species that had not been previously subjected to a full single-laboratory validation scheme. The refined approach was developed following the need to assess performance in a number of shellfish species infrequently monitored through the UK statutory monitoring program, while reducing the impact and cost of the studies, most notably in terms of the use of valuable reference standards. The species assessed were manila clams
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