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Ru₁₁Lu₂₀, a New Intermetallic Compound with Eight- to Ten-Coordinate Ruthenium Atoms

Author： Zimmermann Sina Pantenburg Ingo Meyer Gerd

Publisher： MDPI

E-ISSN： 2073-4352|2|2|704-709

ISSN： 2073-4352

Source： Crystals, Vol.2, Iss.2, 2012-06, pp. : 704-709

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Abstract

The new intermetallic compound Ru₁₁Lu₂₀ was obtained as black single crystals during an attempted comproportionation reaction of lutetium(III) chloride, LuCl₃, with metallic lutetium in the presence of ruthenium metal at 950 °C. Ru₁₁Lu₂₀ crystallizes with the trigonal space group R-3, Z = 6, a = 1255.1(1), c = 2973.0(4) pm, R₁ for all data: 0.0380. Ruthenium atoms center eight-, nine- and ten-vertex polyhedra of lutetium atoms which are connected in a complicated manner to a three-dimensional network.

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