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Mossbauer investigations of corrosion environment influence on Fe valence states in oxide films of zirconium alloys

Author： Filippov V. Petrov V. Shikanova Yu.

Publisher： Springer Publishing Company

ISSN： 0304-3843

Source： Hyperfine Interactions, Vol.167, Iss.1-3, 2006-01, pp. : 747-751

Disclaimer: Any content in publications that violate the sovereignty, the constitution or regulations of the PRC is not accepted or approved by CNPIEC.

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Abstract

Mössbauer investigations about iron atom redistribution in oxide films of zirconium alloys subjected to corrosion at 500°C in pure oxygen and water pair have been analysed. The alloys were also subjected to autoclave conditions at a pressure of 10.0 MPa and autoclave conditions at 350°C and at a pressure of 16.8 MPa, using distilled water and water with additives of lithium and fluorine. It is shown that, depending on the corrosion environment, various compounds of iron, such as α-Fe₂O₃, Fe₃O₄, and FeO, as solid solutions of iron in ZrO₂ are formed in oxide films.

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